In-situ TEM Investigation of Reduction-Oxidation Reactions during Densification of Iron Oxide Nanoparticles
نویسندگان
چکیده
منابع مشابه
In situ UV-visible assessment of extent of reduction during oxidation reactions on oxide catalysts.
The extent of reduction of active centers during oxidative alkane dehydrogenation on VOx/Al2O3 was measured from pre-edge UV-visible spectral features and found to increase with increasing VOx domain size and propane/O2 ratio.
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Iron oxide (Fe2O3) nanoparticles were synthesized by a simple approach using sodium borohydride (NaBH4) and Iron chloride hexahydrate (FeCl3.6H2O). Their physicochemical properties were characterized by high resolution transmission electron microscopy (HRTEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and electron dispersive spectroscopy (EDS). XRD pattern showed that the iron...
متن کاملSynthesis of Iron Oxide Nanoparticles using Borohydride Reduction
Iron oxide (Fe2O3) nanoparticles were synthesized by a simple approach using sodium borohydride (NaBH4) and Iron chloride hexahydrate (FeCl3.6H2O). Their physicochemical properties were characterized by high resolution transmission electron microscopy (HRTEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and electron dispersive spectroscopy (EDS). XRD pattern showed that the iron...
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Oxidation of alloy often involves chemical partition and injection of vacancies. Chemical partition is the consequence of selective oxidation, while injection of vacancies is associated with the differences of diffusivity of cations and anions. It is far from clear as how the injected vacancies behave during oxidation of metal. Using in-situ transmission electron microscopy, we captured unprece...
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ژورنال
عنوان ژورنال: Microscopy and Microanalysis
سال: 2014
ISSN: 1431-9276,1435-8115
DOI: 10.1017/s1431927614009520